Details, Fiction and tga66
Details, Fiction and tga66
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以下因為這次忘記拍照，先用一些示意圖，等之後修理其他支的機會，再來補照片
Then again, the steady multilayer carbonaceous chars (Determine 5) made from your reaction between HCNP and also the decomposition products of PA66 can insulate the underlying substrate in the warmth source and decelerate the two the heat and mass transfer [twenty five]. Therefore, it can be summarized that HCNP can effectively Increase the flame retardancy of PA66 following the gasoline-period flame retardant mechanism.
The microtopography of HCNP is shown in Figure two. The SEM and TEM final results clearly confirmed the HCNP presents a spherical construction, and also the diameter in the HCNP microsphere is about 2 um by using a smooth surface area.
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The microstructure review of your HCNP and char layers shaped during the combustion inside the cone calorimetry check was done utilizing the scanning electron microscope ZEISS Sigma HDTM. Pictures have been received less than vacuum at a voltage of 5 kV.
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PA66 pellets and HCNP powder have been dried for 4 h at a hundred °C ahead of extrusion. The FR-PA66 was ready by twin-screw extrusion response in the range of 260–270 °C. The exam samples have been made employing a TTI-95G injection molding equipment less than 265 °C by using a one hundred eighty r/min rotation speed. Determine six reveals the microtopography of pure PA66, HCNP, and FR-PA66. It could be witnessed from Determine 6c which the HCNP microspheres have been dispersed far more uniformly devoid of apparent phase interfaces, and the peeling phenomenon appeared within the surface area with the microspheres (Figure 6d), indicating that the terminal carboxyl groups of PA66 had been chemically bonded Using the amino teams on the area from the microspheres over the extrusion reaction, which ruined the regularity in the surface area on the microspheres (Figure 6b, easy surface tga66 and no peeling phenomenon) and led for the core–shell separation from the microspheres (Figure 6d), confirming the incidence from the in situ loading reaction.